PhotoCube™ Plus

Advanced Photochemistry in Batch and Flow

Safe and Efficient Photochemistry

 
Built on the legacy of our award-winning PhotoCube™, this new device comes with improvements to better meet the needs of synthetic chemists in the photochemical industry.

The PhotoCube™ Plus provides a reliable cooling function, additional light source customization, and compatibility with ThalesNano fleets – ultimately contributing to reaction scalability and reproducibility.

PhotoCube 2 photochemical reactor

Main features

 

  • Light source: LED, 4 wavelengths in one device
  • Basic configuration: UV (365 nm), blue (457 nm), green (523 nm), red (625 nm)
  • Custom wavelength types are available upon request and easily changeable
  • Seamless control over light intensity through the touchscreen interface
  • Multiple wavelengths can be operated at once
  • Unparalleled safety: automatic lighting shutdown upon opening the device's door
  • Operates in batch and flow mode
  • Batch: magnetic stirring, adjustable stirring speed
  • Cooling: Optional cooler module using cold finger technology, vials can be cooled down to 10 - 15 °C (depending on the type of reaction)
  • Advanced control via the THS ReAction® Software (in-line analytics, manual and automated remote control)

How does it compare to the previous PhotoCube™?

 

Version comparison
PhotoCube™ Plus PhotoCube™
Multiple wavelengths at once? Yes Yes
Number of wavelengths that can be used at once, at high intensity 4 1 (simultaneous use is only recommended at low intensity)
Cooling to room temperature Optional cooler module with built-in cold fingers External fan
User interface Attached to the device External
Compatibility ThalesNano instrument fleets and third-party devices through the THS ReAction® Software Standalone

 

Photochemistry in Flow

 
Photochemistry is a powerful field within organic chemistry that explores the reactions and transformations initiated by light. One notable example is the widely-studied Minisci reaction, which offers a particularly valuable approach for creating new C(sp2)-C(sp3) bonds. However, traditional batch procedures often suffer from lengthy reaction times.

Fortunately, the emergence of continuous flow technology has revolutionized the field of photochemistry. By employing flow reactors, we can significantly accelerate photochemical reactions, enabling faster synthesis processes and streamlined workflows. Moreover, with careful planning, multiple synthetic steps can be seamlessly merged into a single continuous flow sequence, resulting in higher overall yields and increased efficiency.

At ThalesNano, we embrace the power of photochemistry and continuous flow technology to unlock new possibilities in synthesis. Our cutting-edge solutions enable researchers and chemists to harness the benefits of photochemical transformations, achieving remarkable results with enhanced speed, efficiency, and productivity.

Applications

 

  • Bromination
  • C-C coupling
  • Minisci reaction
  • Thiol-ene click reaction
  • Atom transfer radical addition
  • Photocatalytic activity testing
  • Spectrophotometry

Compatible Modules

Knauer HPLC pump >>

10mL/min or 50mL/min capacity pumps with built-in inlet pressure sensors, maintaining a constant flow within the system.

Eldex Optos HPLC pump >>

Up to 80 mL/min capacity pumps with built-in inlet pressure sensors, maintaining a constant flow within the system.

THS System Controller® >>

Enables communication between all connected devices within the fleet. Its software counterpart, THS ReAction® Software, allows for precise operation of the entire fleet from a single screen.

THS RS232-CAN Converter

Designed to connect external modules, such as HPLC pumps, mass flow controllers, and autosamplers to the fleet through the THS System Controller®.

Connect devices of the same type to the THS System Controller

Specifications of the PhotoCube™ Plus

Technical data
Light Source LED
Wavelength types Basic configuration: 365 nm, 457 nm, 523 nm, 625 nm (custom types upon request)
Max. light capacity 24 W/color
Multiple wavelengths at once? Yes (high and low intensity)
Medium temperature at max. LED power 10 - 15 °C with cooler; 40 - 50 °C without cooler
Batch mode 4 x 4 ml or 4 x 30 ml vials; magnetic stirring with adjustable stirring speed
Flow mode 8 ml loop, other loop sizes on request, flow rate: 0.1 – 10 ml/min
Cooling Cooler module with cold finger technology
Dimensions (H x W x D) 270 x 244 x 420 mm
Dimensions without the cooler module (H x W x D) 200 x 244 x 420 mm
Mains voltage 110 – 230 V AC, 50 – 60 Hz
Power input device: 12 V, 150W; cooler: 12 V, 250W
Unit weight 12 kg (with the cooler module)

Do you have more questions?

 
Reach out to us at any time and experience fast and efficient support tailored to your specific needs.